2024 Capability Portfolio Digital | Page 34

Clean Energy Capability Portfolio | Renewable Generation

X-Ray Capabilities for

Characterisation of
Energy Materials and
Devices

X-rays are high energy , penetrating light with wavelengths around the length of atomic bonds , which gives them unique properties for exploring energy materials . Our experienced team of twelve instrument scientists can assess chemistry , surfaces , mineralogy and high-resolution 3D images of energy materials and devices for research or industry , often under dynamic conditions during operation .

Competitive Advantage

• Largest combined X-ray laboratory in Australia offering an unparalleled range of instrument capabilities and technical expertise – XRD , TF-XRD , SC-XRD , XPS , XRF , micro-XRF , XPS , micro-CT , EXAFS
• Easy access and support for enquiries , problem solving , multi-technique projects , training , and professional administrative services

Impact

• Deeper understanding cell performance during charge-discharge cycling by monitoring changes in solid electrolyte mineral phases in operando
• Fine-tuning hydrogen-storage in molecular framework materials
• Optimising surface chemistry of graphite-coated electrodes
• Confirming chemistry and structure of thinfilm multilayer semiconductors ( e . g ., thin-film photovoltaics )

Capabilities and Facilities

• Mineralogy and molecular structure – X-ray diffraction of bulk solids and thin-films and crystals
• Chemistry – X-ray fluorescence of bulk solids from % to ppm
• Surfaces – X-ray photoelectron spectroscopy for chemistry at the top 5 nm , or nanoscale depth profiling
• 2D Imaging – X-ray fluorescence microscopy down to 20mm under inert gas or vacuum
• 3D Imaging – micro-CT with helical and circular scanning mode with pressure and flow cells for various sample sizes and image processing support

More Information

Dr Christopher Marjo
Mark Wainwright Analytical Centre
Solid State and Elemental Analysis Unit
T : + 61 434 181 790

Successful Applications

E : c . marjo @ unsw . edu . au
• Quality assessment of new and used electrode surfaces / subsurfaces
• Supporting the development of record-breaking thinfilm photovoltaics
• Troubleshooting automotive cells and batteries using 3D imaging

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