UHP Gases Issue 02 | Page 14

TECHNOLOGY FOCUS EXPERT FOCUS INSIDE THE COULOMETRIC OXYGEN SENSOR A COMBINED SOLUTION FOR YOUR UHP GAS PROCESS PROVIDING A COMPREHENSIVE, SINGLE-SUPPLIER SOLUTION FOR YOUR UHP PROCESS – FROM PRECISION GAS ANALYSIS TO ENTIRE SYSTEMS AND EXPERT GLOBAL SUPPORT Servomex’s non-depleting Hummingbird Coulometric sensor technology is at the heart of our high-purity oxygen analyzer range. It enables direct measurements at trace and ultra-trace levels, without the requirement for periodic replacement or false low readings associated with fuel cell sensors. The sensor operates on a simple coulometric process whereby oxygen in the sample gas is reduced in an electrochemical reaction. The sample gas is in direct contact with the sensor cathode. Discover our analyzer range: servomex.com/gas-analyzers Oxygen (O 2 ) in the sample gas is reduced electrochemically at the cathode to hydroxyl ions (OH - ). The electrolyte solution contains potassium hydroxide (KOH) which assists in the migration of OH - to the high-purity, non-carbon anode, where they are oxidized to complete the reaction. Servomex’s analyzer range is the most comprehensive available from a single manufacturer, setting the standard for the ultra-high-purity (UHP) gas market for decades with a unique ‘all of market’ solution. A voltage of approximately 1.3V DC, applied to the sensor electrodes, drives the reduction and oxidation reactions. The current flow resulting from the reaction is proportional to the oxygen content in the sample gas. The processed signal is then displayed on the front panel in parts- per-million (ppm) or parts-per-billion (ppb) units of O 2 . This provides a direct measurement for O 2 , eliminating the errors that inevitably result from technologies that measure the O 2 content indirectly. Powered by reliable, ground-breaking sensor technologies, our range delivers accurate, stable measurements for every point in your process, with a full range of percent to ultra-trace measurements. Servomex analyzers support quality control, maintaining gas purity during the production process and detecting impurities during processes such as medical gas supply or semiconductor production. We also provide solutions for process control and ensure safety and emissions monitoring for potentially hazardous processes. Our commitment to ongoing development ensures that even the most trusted measurements are continuously improved, with added features that increase ease of use and reduce the cost of ownership. The Coulometric sensor also responds very quickly to changing O 2 concentrations: the 0-1,000ppm range sensor can be exposed to air and in less than a minute will measure <10ppm on pure nitrogen – beneficial for users who have upset-prone applications. Discover our systems solutions: In addition to fast response to changes in O 2 concentration, the performance of the sensor is unaffected by reasonable changes in flow rate. Because the non-depleting sensor is not consumed when exposed to O 2 , it has a long lifespan and does not require a purge gas to protect it when it's not in use. Coulometric sensing complements Paramagnetic oxygen sensing by being able to measure ppm level measurements, where Paramagnetic lacks sensitivity at these levels. There are some limitations however: the sensor cannot be used with gases containing alcohols, aldehydes and solvents. DF-550E servomex.com/systems 10 6. DF-560E 5m mm m 96.5 In addition to individual analyzers, Servomex also supplies complete system solutions designed to order for your project. State-of-the-art systems engineering centers in the US, China, India and Europe provide a global service, offering solutions ranging from simple utilities panels to fully-contained air- conditioned shelters. Proven experience ensures the optimum level of efficiency, safety and cost- effective operation for your application. DF-760E Discover our service solutions: Delivering ultra-trace measurements of O 2 as a contaminant in UHP electronic gases, the DF-550E’s fast response and highly-sensitive 200ppt Lower Detection Limit (LDL) provides dependable process monitoring. Find out more: see page 18 P14 Designed to measure ultra-trace O 2 to an industry-leading 45ppt LDL, the DF-560E delivers a fast-response measurement in multiple background gases. Find out more: see page 18 Providing a unique, simultaneous dual measurement for trace moisture and trace O 2 , the DF-760E is a compact solution for monitoring UHP bulk gases in integrated circuit board manufacture. Find out more: see page 21 servomex.com/service-network Servomex support doesn’t end with the supply of your analyzer or system. Our expert team delivers gas analysis expertise directly to your plant. With global coverage provided by service centers and mobile engineers worldwide, the Servomex Service Network ensures your processes run efficiently, safely and profitably. Support offered includes service contracts, spares, calibration kits, commissioning, health checks, training, and equipment rental. We also provide expert support from our extensive network of service centers, or on-site at your facility. P15