Industrial Gases Issue 01 | Page 8

SOLDER REFLOW FURNACES THE SERVOPRO MonoExact DF310E AND AquaXact 1688 WORK TOGETHER TO PROVIDE A COMPLETE GAS AND MOISTURE ANALYSIS SOLUTION FOR FURNACE ENVIRONMENTS TRACE MEASUREMENTS FOR FURNACE ENVIRONMENTS While the SERVOPRO MonoExact DF310E digital oxygen analyzer can use both Coulometric and Paramagnetic sensing technology to measure O 2 , the relevant technology for this process is Coulometric. Coulometric process which sees O 2 in the sample gas reduced at the cathode to hydroxyl ions. Assisted by a potassium hydroxide electrolyte, the ions migrate to the anode, where they are oxidized back to O 2 and vented out of the sensor. Conventional electrochemical sensors use a consumable lead anode and silver cathode. The carbon/nickel composition Using carbon and nickel electrodes which remain unaffected by chemical change, the non-depleting Coulometric sensor avoids the problems associated with galvanic or zirconium oxide sensors in a furnace. of the Coulometric electrodes means they are non-depleting. Neither electrode undergoes chemical change, so excellent measurement stability is achieved. Coulometric sensing also provides a fast response, giving an immediate indication of any changes in O 2 , regardless of whether that change is caused by an ambient air leak or by incorrect N 2 inerting levels. ACID GAS TOLERANCE RAPID RESPONSE Unlike those sensor technologies, the Coulometric sensor does not need periodic replacement, nor does it produce false low readings due to a loss of measurement sensitivity or a reaction with sample gas components. It also offers an advantage over galvanic sensors by not needing frequent calibrations. The way the sensor works is by a simple ALUMINUM OXIDE The ability of the SERVOPRO MonoExact DF310E and AquaXact 1688 to integrate seamlessly for the combined analysis of O 2 and moisture offers an ideal solution for many applications, including metals annealing, air separation, instrument air production and glove box purging. One specific application is solder furnace monitoring, which requires careful, responsive, and accurate control of oxygen and moisture in the furnace environment. In the past, printed circuit boards (PCBs) were cleaned with chlorofluorocarbon (CFC) based agents before soldering. However, the use of CFCs has now been largely eliminated because of environmental concerns. This means PCB manufacturers must create an inert environment in the solder furnace. To ensure consistent soldering quality, it is necessary to monitor the level of O 2 in the furnace. P08 If high-quality solder joints are to be assured, the nitrogen in the solder furnace also needs to have a low moisture dew point, typically below -50 o C. Servomex’s MonoExact DF310E digital oxygen analyzer uses Coulometric sensing technology to measure ppm O 2 . This Coulometric sensor needs only an annual span adjustment, bi-annual addition of replenishment solution, and no proactive maintenance cell replacements, all of which lowers the lifetime cost of ownership. It also offers a five-year performance guarantee not matched by any other oxygen analyzer company. Adding the AquaXact 1688 to the MonoExact DF310E’s digital electronics provides an ideal solution for the exceptionally accurate monitoring of both O 2 and moisture in one system. Unlike conventional moisture sensors, the AquaXact 1688 does not suffer from drift, so the response curve remains the same even after many months of operation at an elevated temperature. In solder furnaces, this combination of technologies means excellent batch-to- batch solder quality and significantly reduced nitrogen consumption, with no compatibility issues caused by using sensors from different sources. Aluminum Oxide sensors work by measuring the capacitance between the aluminum core and a gold film deposited on top of the oxide layer. This varies with the water vapor content contained in the pores of the oxide layer. Three fundamental structural improvements in the oxide layer mean that the AquaXact 1688 has industry- leading sensitivity and stability. Firstly, the Servomex sensors have a much thinner oxide layer than comparable devices, without compromising transmitter strength. Since capacitance is inversely proportional to the distance between the capacitor’s plates, the GAS SAMPLE CARBON CATHODE 40H - NON DEPLETING PROPRIETARY ANODE O 2 Coulometric sensing O 2 + 2H 2 O + 4e - 4OH - (cathode) 4OH - O 2 + 2H 2 O + 4e - (anode) thinner layer produces much higher capacitance changes, reducing the impact of drift due to undesirable factors. capacitance for a given change in dew point is increased, providing more accurate results, and a quicker response. It also means water moves in and out of the pores more quickly, producing a faster response than conventional Aluminum Oxide sensors. The pore geometry in conventional sensors collapses slowly over time, requiring frequent recalibration. The AquaXact 1688’s pore geometry does not change significantly, so it needs only an annual calibration check when used in clean, non-corrosive gases. A better-defined barrier layer between the aluminum and the aluminum oxide reduces metal migration, which is one of the major causes of aging drift in conventional sensors. The response curve for the AquaXact 1688 is unchanged by several months of operation at a high temperature. The most significant improvement is the unique, stable pore geometry of the AquaXact 1688, which enhances the entrapment of water molecules. By holding more water, the change in ct DF310E The combination of MonoExa an ideal and AquaXact 1688 is also ting solution in metal heat trea ire accurate requ also ch whi , ions licat app e. stur moi and O 2 of monitoring Get the combined solution for your process today: MonoExact DF310E: servomex.com/monoexactdf310e AquaXact 1688: servomex.com/aquaxact1688 P09