Industrial Gases Issue 01 | Page 22

AIR

CRYOGENIC AIR SEPARATION

The process begins with the air being filtered and compressed to remove dust. The air is then cooled and purified, generally through a series of filters, to remove water vapor, carbon dioxide and gaseous hydrocarbons.
Next, the air is passed through an integrated heat exchanger and cooled to around-180 o C cryogenically. Part of the
air is liquefied, to form a liquid rich in oxygen, while the remaining gas is much richer in nitrogen.
This mixture of liquid and vapor air is then separated and fed to a separation column – consisting of a high pressure and low pressure column, where the mixture is then separated into oxygen, nitrogen and argon streams.
Gas analyzers are required to provide continuous and reliable measurements throughout the process. Alongside analysis of the quality of the produced gases themselves, safety and control measurements may be required to monitor the levels of carbon dioxide, nitrous oxide, hydrocarbons, water vapor and trace impurities.
LOCAL PIPELINE USERS
PRODUCT COMPRESSION
GAR
GAN
GOX
MonoExact DF310E / MultiExact 5400, Chroma 0-1 / 10ppm 0-10ppm 90-100 % O 2 Impurities Ar
MonoExact DF310E / MultiExact 5400, Chroma 0-1 / 10ppm 0-10ppm O 2 Impurities
MultiExact 5400, FID, Chroma 98 %-100 % 0-10ppm O 2 CO 2 THC Impurities Ar
MAIN HEAT EXCHANGERS COLD BOX
WARM
WARM
NITROGEN
GAN
MultiExact 5400, MultiExact 4100 0-20 % O 2
MultiExact 5400, FID 0-100ppm 0-10 / 100ppm CO 2 THC
COOL
INTERNAL REFRIGERATION OF LIQUEFIER COLD BOX
CO‘ CO
AIR FEED
FILTER
FID Chroma 0-10 / 100ppm THC Impurities
PPU
( MOLE SIEVE)
OXYGEN
MultiE MultiE FID 98 %-1 0-2 0-1 O 2 CO 2 N
COMPRESSOR
LIQUID H 2 O
GASEOUS
H 2 O, CO 2, HC IMPURITY REMOVAL
PARTIALLY CONDENSED
CR DIS
P12