IM 2018 March 18 | Page 48

MINE WATER MANAGEMENT their water management appears to be increasing. With the increasing stringency of discharge permits, advanced technologies and regulators demanding that a WTP is online before any mining activity commences, the value of efficient and expert execution has become paramount. Fighting calcium sulphate A North American multi-metal mining operation began experiencing severe, tenacious calcium sulphate deposition in its leaching operation shortly after coming on-line. It was reconfigured to incorporate a thickener as an additional clarifier to reduce scale formation and promote precipitation of calcium sulphate. Calcium sulphate deposition at the mine site was difficult to address because the process water pH was highly acidic, typically 1-2. Many deposit control chemistries are ineffective at this low pH. The low pH and use of seawater for process water also made assessment of antiscalant program performance difficult. Low pH is corrosive to mild steel, and seawater is corrosive to stainless steel, making it difficult to use traditional scale coupons to monitor the results of deposit control programs. The thickener reconfiguration resulted in a copper production loss of some 6%. The mine lost additional productivity from reduced flows and periodic cleaning shutdowns due to scale build up in the process lines and equipment. The mine wanted to reduce or eliminate scale formation in the leach circuit and be able to monitor program performance. ChemTreat laboratory and technical personnel worked with the mine’s metallurgical group to screen potential antiscalants, leading to the development of ChemTreat ML708 scale and deposit control agent. ChemTreat then designed and fabricated scale coupons made of titanium and fibreglass that were effective at low pH and in seawater. Finally, ChemTreat developed a pilot unit that assessed the process water flow and scale formation both before and after the injection of ChemTreat ML708 to validate the antiscalant program’s performance. Baseline data prior to the ML708 antiscalant addition revealed a calcium loss of 2.5% through the leach circuit, which translated to a daily precipitation of approximately 2 t of calcium sulphate. The coupons also showed rapid scale build up. Application of ChemTreat ML708, however, consistently kept the calcium in solution throughout the circuit, as evidenced by clean coupons and the mine’s ability to operate without interruption during the initial month-long program evaluation. The pilot unit also verified the efficacy of ML708 in preventing scale formation. ChemTreat ML708 proved effective in inhibiting 46 International Mining | MARCH 2018 calcium sulphate scale formation under the acidic and highly- ionic conditions of the mine’s process water. Its unique chemistry allows it to function in operations where commonly-used antiscalant polymers show limited or no success in controlling scale because of low pH or high brine strength. ChemTreat designed and built retractable titanium and fibreglass scale coupons. Calcium analyses performed by the mine’s laboratory validated the antiscalant program’s ability to maintain calcium concentration across the leach circuit. The ChemTreat team met the mine’s objectives to reduce calcium scale in their operation and monitor and validate the performance of the program. Maximising membrane plant efficiency Genesys International is also at the forefront of fighting calcium sulphate and other scale deposits, but specifically in reverse osmosis and nanofiltration membrane plants fed with mine water. Membrane technology is being adopted widely by mines, both to clean up and reuse wastewater and to concentrate metals for enhanced recovery. There are now more than 300 membrane plants treating mine water around the world. In 2017, Genesys won a £500,000 research grant from Innovate UK – a UK Government industrial initiative – specifically to fund investigations into the scaling that affects membrane plants used to manage mine water and how to tackle it. Genesys first started looking seriously into how its products could help in the mining industry back in 2012, when the company discovered that large orders for one of its products from Peru were being used at gold mines. Mine operators had chosen Genesys Calcium Sulphate Antiscala nt (CAS) based on independent studies, which had shown it was the most effective product for inhibiting calcium sulphate scale from reverse osmosis membranes. Fernando del Vigo of Genesys Spain paid several visits to the Peruvian mines to monitor and optimise their antiscalant use and conduct membrane autopsies and cleaning tests. The sheer volume of Genesys CAS orders from various countries prompted MD, Steve Chesters, to investigate further, and he discovered that products were already being used at mines With the help of an Innovate UK grant, Genesys has developed mine water scaling prediction software specific to the mining industry. The funding is also helping it rewrite the chemistry book for the extremes of pH and scale formation that occur in mining applications. Here testing is underway in a pilot plant rig around the world. So, in 2016 Genesys took the step of employing Phil Morton as Mining Manager. He had previously worked at Glencore’s Mount Isa mines and Barrick’s joint venture mine in Saudi Arabia. “The complexity of mining water chemistry means each mine and reverse osmosis membrane plant has different requirements,” says Morton. “Because Genesys is uniquely set up to conduct membrane autopsies and run scaling tests, we can formulate site-specific antiscalants for any mine in the world.” Max Fazel, Senior Research Chemist at the Genesys R&D centre in the UK, has been conducting a series of tests and experiments to gain greater understanding of calcium sulphate solubility in various conditions. “The solubility of calcium sulphate is very different at acidic pH than at alkaline or neutral pH,” he explains. “This means we need to formulate, test and prove specific antiscalants for use in membrane systems in situations where calcium sulphate scale is a problem.” Genesys has already developed tailored products for different mines in Peru and has recently specially created one for a mine in Australia which suffers from high levels of barium and silica scaling. “Conventional reverse osmosis antiscalants simply don’t work at these extremes,” says Chesters. “With the new products and software we’re developing, we’re optimistic that we can help to make reverse osmosis a viable option for more mines, enabling them to clean up dirty water and extract precious metals more efficiently.” Morton adds, “Our research has made it clear that no single product would work for all mine waters. They are as unique and changeable as the orebodies being mined. Running synthesised