Bulk Distributor Nov/Dec19 | Page 8

8 B ULK D ISTRIBUTOR Cleaning & Repair November/December 2019 The pitfalls in pitting T he recent TT Club seminar on Managing risk for tank containers (see p 4) included a technical paper of great relevance to repair depots. Dr Ken Kirby, Ronald Veen and Arron Jackaman, of Brookes Bell discussed Practical problems faced when tank containers experience pitting. They began by listing what the actual condition of a tank is likely to be. It is often the case that there is limited information on cleaning and maintenance programmes. Passivity and roughness records are rarely kept if in existence at all. In the event of damage to a container the easiest option is to select the most recent cargo as the cause. However, it is sometimes the case that the condition of the stainless steel within the tank was poor, but the lack of information regarding the tank surface condition means it is difficult to determine fault. They then detailed the condition the tank container should be in on delivery. The stainless steel needs to be clean, ie, free from visible stains and dirt, and smooth, with an Ra value under 1.5mm. But critically it also needs to be passive. As per the oxilyser3 test (a stainless steel passivity tester), a value above 65, or preferably higher, is required. Passivity is a property of the stainless steel to resist corrosion under conditions where it should otherwise corrode. A common misconception is that stainless steel is stainless, but this is not true as stainless steel can be readily tainted by cargo residues (resulting in a varnish). It can also suffer from rouging under certain conditions. Another form of staining commonly observed is ‘tea- staining’, which is caused by surface contamination. Cleaning can be carried out by chemical means; but in extreme cases chemical cleaning is not sufficient and mechanical cleaning (polishing) becomes necessary. The surface condition should be as smooth as possible to have a positive effect on future cleaning regimes. Improvements in surface roughness also enhance corrosion resistance. delivered to the depot, an estimator visually accesses the condition of the tank and may request an area of test grinding – this might be supported by non-destructive testing (NDT) such as a dye penetrant. If significant pitting is found the assessor may request for a small area to be test ground to check physically how deep the pits are in the test area. This is then used to help determine the likely time required for repairs to the whole tank. Repairs are then conducted by grinding and polishing and should be followed by pickling and passivation. Pitfalls Within the pit aggressive ions accumulate combining with hydrogen forming acidic species But the speakers said their experience is that surface roughness condition is often ignored, because operators underestimate the significance. In fact, surface roughness will deteriorate over time and so should be monitored regularly. If the surface becomes rough then the remedial action is to grind and polish (ie, buffing). They then moved onto pickling and passivation. Pickling is the removal of the metallic dirt and the damaged oxide (passive) layer. This removes light discolouration and tarnish – particularly heat-tint after welding – and also aids the promotion of beneficial elements to the surface resulting in improvements to corrosion resistance. Passivation is the formation of a new oxide layer by chemical means. So what happens in practice? When an off-hire tank container is But there are pitfalls in the repair process. The estimator has no realistic idea (even though experience will help to some extent) how deep the pits are, and it is often the case that the test area does not accurately represent the remainder of the tank. It is also the case that some areas can be so badly pitted that repair/remedial action is uneconomical – this won’t be known until grinding happens and sometimes long in to the repair process. This results in wasted costs for the operator. Improvements can be made, however. For example, checking the cleaning and repair processes by an expert, and also performing stainless steel surface testing in regards to surface roughness, ferrous contamination and passivity in order to prevent as much as possible the pitting corrosion. To get a correct understanding about pickling and passivation it is necessary first to be aware that the difference between pickling and passivation is like salt and sugar. For instance, is pickling required after surface grinding and polishing, or will passivation only have a better effect? Brookes Bell has observed at tank repair depots that people are referring to pickling and passivation, but in fact they only carried out pickling without chemical passivation, while it should be chemically passivated in order to reach its desired strong passive oxide layer to